Memory effects on crystallization behaviours of poly(l
Memory effects play an important role in understanding polymer crystallization especially for self-seeding or self-nucleation of polymer crystallization. Amorphous poly (L -lactic acid) (PLLA) was prepared via quenching after holding at various temperatures.
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Under certain conditions such as low temperature storage the dissolved KHT becomes insoluble and small crystals settle to the bottom in the form of sediment. In a supersaturated solution (e.g. wine) the crystallization process occurs in two stages. In the first stage also referred to as the nucleation phase nuclei or seed crystals are formed.
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bution in crystallization is mostly made during the seeding period. The seeding under tech-nical conditions remains a critical step which deserves optimization. Optimal seeding con-ditions followed by minimizing secondary nu-cleation throughout the crystallization cycle are needed. The optimal quantity of seed crystals needs to be determined.
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In a cooling crystallization this might be referred to as the "seeding temperature" but it is actually the supersaturation level that is being considered. Seeding at high supersaturation levels may result in excessive secondary nucleation rendering the seeding process itself redundant unless the goal is a fine crystal size distribution.
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Seeding with α‐Al 2 O 3 lowered the α‐Al 2 O 3 crystallization temperature in these xerogels by 100° to 150°C. Spinel seeds have much less effect on the γ‐α transition and α‐Fe 2 O 3 and SiO 2 seeds do not affect it significantly. Isostructural seeding of gels may therefore permit lower ceramic processing temperatures.
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Jan 01 1991 · The role of solid state epitaxy in the crystallization of nanocomposite cordierite glass to glass ceramic was investigated. The use of isostructural (α-cordierite) seeds in cordierite glass led to a lowering in the crystallization temperature to form glass ceramic by about 50 °C compared to the unseeded glass. The use of non-isostructural seeds such as ZrO2 and TiO2 did not lower the
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How to Grow Crystals. The idea is to grow a single crystal not a bunch of crystals. You will first need to grow a small perfect crystal your seed crystal around which you will later grow a large crystal.It is therefore essential to avoid excessive rapid growth which encourages the formation of multiple crystals instead of a single crystal.
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Seeding with α‐Al 2 O 3 lowered the α‐Al 2 O 3 crystallization temperature in these xerogels by 100° to 150°C. Spinel seeds have much less effect on the γ‐α transition and α‐Fe 2 O 3 and SiO 2 seeds do not affect it significantly. Isostructural seeding of gels may therefore permit lower ceramic processing temperatures.
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In this work the effect of crystallization parameters i.e. supersaturation seeding and temperature on the polymorphism and crystal size of a nonsteroidal anti-inflammatory drug indomethacin (IMC) was investigated. First several crystallization solvents (ethanol methanol ethyl acetate acetone acetonitrile and dichloromethane) were screened through the measurement of IMC solubility
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Again this seed crystal acts as a template on which the dissolved solid will begin crystallizing. If neither of these two techniques results in crystallization the compound was probably dissolved in too much hot solvent. and then allow the solution to cool to room temperature again to effect crystallization.
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adshelp at cfa.harvard.edu The ADS is operated by the Smithsonian Astrophysical Observatory under NASA Cooperative Agreement NNX16AC86A
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Mar 17 2015 · Table 1 contains the minimum KCP values observed for wines stored at three temperatures for 21 days1 without adding KHT seed crystals. If a dry Chardonnay wine has a KCP value of 14.6 x 10 -5 or lower it should usually be cold stable to 5° C. Temperature may be estimated when the KCP value falls between those listed in Table 1.
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In this work the effect of crystallization parameters i.e. supersaturation seeding and temperature on the polymorphism and crystal size of a nonsteroidal anti-inflammatory drug indomethacin (IMC) was investigated. First several crystallization solvents (ethanol methanol ethyl acetate acetone acetonitrile and dichloromethane) were screened through the measurement of IMC solubility
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Start of temperature control program Addition of seed crystals 3 70 min While crystallization is running Review of theory with the assistant 4 30 min the seed crystals are mono disperse i.e. all seed crystals have the same size The balance equation for such a
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HOW CAN WE DETERMINE THE EFFECTS OF SEEDING Seeding effects and benefits can be demonstrated in a number of ways. The most direct method is to conduct a project over several years in which half of the storms are randomly seeded and the resulting precipitation from the seeded and unseeded storms is compared. From The Wyoming Weather
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effects from cloud seeding with silver iodide. Background The vast majority of modern attempts at modifying weather involve cloud seeding which is the intentional treatment of individual clouds or cloud systems to achieve a desired effect (WMA 1996). As the second driest state in the U.S. the goal of cloud seeding programs in Utah has
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Increasing precipitation requires one of two approaches to help water particles collide merge and grow glaciogenic seeding and hygroscopic seeding. Glaciogenic seeding uses agents such as silver iodide that initiate ice formation in "cold clouds " those colder than 0 °C and that have supercooled water.
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Mar 17 2016 · The government didn t quietly admit to modifying weather in California cloud seeding is a well-documented effort to counteract the effects of drought (and isn t related to chemtrails
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Under certain conditions such as low temperature storage the dissolved KHT becomes insoluble and small crystals settle to the bottom in the form of sediment. In a supersaturated solution (e.g. wine) the crystallization process occurs in two stages. In the first stage also referred to as the nucleation phase nuclei or seed crystals are formed.
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Under certain conditions such as low temperature storage the dissolved KHT becomes insoluble and small crystals settle to the bottom in the form of sediment. In a supersaturated solution (e.g. wine) the crystallization process occurs in two stages. In the first stage also referred to as the nucleation phase nuclei or seed crystals are formed.
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May 15 2015 · Crystallization is followed on the single-particle level. We investigated a colloidal model system in which the mismatch between seed-induced and
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In this study the memory effect of a polymer is investigated with a mesomorphic isotactic polypropylene (iPP) melt as the initial state. It is found that the nucleation density and crystallization rate at low temperatures are strongly dependent on the initial melting temperature and melting time indicating a strong memory effect. High melting temperatures decrease the nucleation density
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HOW CAN WE DETERMINE THE EFFECTS OF SEEDING Seeding effects and benefits can be demonstrated in a number of ways. The most direct method is to conduct a project over several years in which half of the storms are randomly seeded and the resulting precipitation from the seeded and unseeded storms is compared. From The Wyoming Weather
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Whether you are tempering chocolate making caramel or churning ice cream cooks need to be masters of crystals. In this article food scientist Shirley Corriher tackles the subject of how crystals form. She explains what you need to do to encourage or discourage crystal formation and how to use crystals to control candy texture.
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Whether you are tempering chocolate making caramel or churning ice cream cooks need to be masters of crystals. In this article food scientist Shirley Corriher tackles the subject of how crystals form. She explains what you need to do to encourage or discourage crystal formation and how to use crystals to control candy texture.
Get PriceMethods for Tartrate Stabilization of Wine Midwest Grape
Under certain conditions such as low temperature storage the dissolved KHT becomes insoluble and small crystals settle to the bottom in the form of sediment. In a supersaturated solution (e.g. wine) the crystallization process occurs in two stages. In the first stage also referred to as the nucleation phase nuclei or seed crystals are formed.
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Raising the rewarm temperature had the effect of destroying seed nuclei but this was a more gradual process. The bimodal nature observed of the melting points compared to the more spread-out behavior of crystallization temperatures reflects the kinetic constraints found in crystallization
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The "seed" is tempered chocolate in hunks wafers or grated bits. It is added at the beginning of the tempering process. These crystals of tempered chocolate act like magnets attracting the other loose crystals of fatty acids to begin the crystallization process that results in well-tempered chocolate
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The U.K.-based luxury company Oliver s Travels has announced a weather-modification service that would burst clouds and guarantee clear skies by using cloud seeding a process that encourages
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